A novel wet polymeric precipitation synthesis method for monophasic β-TCP

I. Grigoraviciute-Puroniene, K. Tsuru, E. Garskaite, Z. Stankeviciute, A. Beganskiene, Kunio Ishikawa, A. Kareiva

Research output: Contribution to journalArticle

5 Citations (Scopus)

Abstract

β-Tricalcium phosphate (β-Ca3(PO4)2, β-TCP) powders were synthesized using wet polymeric precipitation method for the first time to our best knowledge. The results of X-ray diffraction analysis showed the formation of almost single a Ca-deficient hydroxyapatite (CDHA) phase of a poor crystallinity already at room temperature. With continuously increasing the calcination temperature up to 800 °C the crystalline β-TCP was obtained as the main phase. It was demonstrated that infrared spectroscopy is very effective method to characterize the formation of β-Ca3(PO4)2. The SEM results showed that β-Ca3(PO4)2 solids were homogeneous having a small particle size distribution. The β-TCP powders consisted of spherical particles varying in size from 100 to 300 nm. Fabricated β-TCP specimens were placed to the bones of the rats and maintained for 1–2 months. The histological properties of these samples will be also investigated.

Original languageEnglish
Pages (from-to)2325-2331
Number of pages7
JournalAdvanced Powder Technology
Volume28
Issue number9
DOIs
Publication statusPublished - Sep 1 2017

Fingerprint

Powders
Hydroxyapatite
Particle size analysis
Calcination
X ray diffraction analysis
Rats
Infrared spectroscopy
Bone
Phosphates
Durapatite
Crystalline materials
Temperature
Scanning electron microscopy
beta-tricalcium phosphate
tricalcium phosphate

All Science Journal Classification (ASJC) codes

  • Chemical Engineering(all)
  • Mechanics of Materials

Cite this

Grigoraviciute-Puroniene, I., Tsuru, K., Garskaite, E., Stankeviciute, Z., Beganskiene, A., Ishikawa, K., & Kareiva, A. (2017). A novel wet polymeric precipitation synthesis method for monophasic β-TCP. Advanced Powder Technology, 28(9), 2325-2331. https://doi.org/10.1016/j.apt.2017.06.014

A novel wet polymeric precipitation synthesis method for monophasic β-TCP. / Grigoraviciute-Puroniene, I.; Tsuru, K.; Garskaite, E.; Stankeviciute, Z.; Beganskiene, A.; Ishikawa, Kunio; Kareiva, A.

In: Advanced Powder Technology, Vol. 28, No. 9, 01.09.2017, p. 2325-2331.

Research output: Contribution to journalArticle

Grigoraviciute-Puroniene, I, Tsuru, K, Garskaite, E, Stankeviciute, Z, Beganskiene, A, Ishikawa, K & Kareiva, A 2017, 'A novel wet polymeric precipitation synthesis method for monophasic β-TCP', Advanced Powder Technology, vol. 28, no. 9, pp. 2325-2331. https://doi.org/10.1016/j.apt.2017.06.014
Grigoraviciute-Puroniene I, Tsuru K, Garskaite E, Stankeviciute Z, Beganskiene A, Ishikawa K et al. A novel wet polymeric precipitation synthesis method for monophasic β-TCP. Advanced Powder Technology. 2017 Sep 1;28(9):2325-2331. https://doi.org/10.1016/j.apt.2017.06.014
Grigoraviciute-Puroniene, I. ; Tsuru, K. ; Garskaite, E. ; Stankeviciute, Z. ; Beganskiene, A. ; Ishikawa, Kunio ; Kareiva, A. / A novel wet polymeric precipitation synthesis method for monophasic β-TCP. In: Advanced Powder Technology. 2017 ; Vol. 28, No. 9. pp. 2325-2331.
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