Abstract
We applied multiple relayed COSY and 2D homonuclear Hartman-Hahn spectroscopy to globoside, a glycolipid purified from human red blood cells. The subspectra corresponding to individual sugar components were extracted even from overlapping proton resonances by taking the cross sections of 2D spectra parallel to the F2 axis at anomeric proton resonances, so that unambiguous assignments of sugar proton resonances were accomplished.
| Original language | English |
|---|---|
| Pages (from-to) | 91-97 |
| Number of pages | 7 |
| Journal | FEBS Letters |
| Volume | 212 |
| Issue number | 1 |
| DOIs | |
| Publication status | Published - Feb 9 1987 |
| Externally published | Yes |
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All Science Journal Classification (ASJC) codes
- Biophysics
- Structural Biology
- Biochemistry
- Molecular Biology
- Genetics
- Cell Biology
Cite this
Analysis of NMR spectra of sugar chains of glycolipids by multiple relayed COSY and 2D homonuclear. Hartman-Hahn spectroscopy. / Inagaki, F.; Kohda, D.; Kodama, C.; Suzuki, A.
In: FEBS Letters, Vol. 212, No. 1, 09.02.1987, p. 91-97.Research output: Contribution to journal › Article
}
TY - JOUR
T1 - Analysis of NMR spectra of sugar chains of glycolipids by multiple relayed COSY and 2D homonuclear. Hartman-Hahn spectroscopy
AU - Inagaki, F.
AU - Kohda, D.
AU - Kodama, C.
AU - Suzuki, A.
PY - 1987/2/9
Y1 - 1987/2/9
N2 - We applied multiple relayed COSY and 2D homonuclear Hartman-Hahn spectroscopy to globoside, a glycolipid purified from human red blood cells. The subspectra corresponding to individual sugar components were extracted even from overlapping proton resonances by taking the cross sections of 2D spectra parallel to the F2 axis at anomeric proton resonances, so that unambiguous assignments of sugar proton resonances were accomplished.
AB - We applied multiple relayed COSY and 2D homonuclear Hartman-Hahn spectroscopy to globoside, a glycolipid purified from human red blood cells. The subspectra corresponding to individual sugar components were extracted even from overlapping proton resonances by taking the cross sections of 2D spectra parallel to the F2 axis at anomeric proton resonances, so that unambiguous assignments of sugar proton resonances were accomplished.
UR - http://www.scopus.com/inward/record.url?scp=0023145334&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=0023145334&partnerID=8YFLogxK
U2 - 10.1016/0014-5793(87)81563-6
DO - 10.1016/0014-5793(87)81563-6
M3 - Article
C2 - 3803612
AN - SCOPUS:0023145334
VL - 212
SP - 91
EP - 97
JO - FEBS Letters
JF - FEBS Letters
SN - 0014-5793
IS - 1
ER -