Analysis of NMR spectra of sugar chains of glycolipids by multiple relayed COSY and 2D homonuclear. Hartman-Hahn spectroscopy

F. Inagaki; D. Kohda; C. Kodama; A. Suzuki

doi:10.1016/0014-5793(87)81563-6

Analysis of NMR spectra of sugar chains of glycolipids by multiple relayed COSY and 2D homonuclear. Hartman-Hahn spectroscopy

F. Inagaki, D. Kohda, C. Kodama, A. Suzuki

Research output: Contribution to journal › Article › peer-review

30 Citations (Scopus)

Abstract

We applied multiple relayed COSY and 2D homonuclear Hartman-Hahn spectroscopy to globoside, a glycolipid purified from human red blood cells. The subspectra corresponding to individual sugar components were extracted even from overlapping proton resonances by taking the cross sections of 2D spectra parallel to the F₂ axis at anomeric proton resonances, so that unambiguous assignments of sugar proton resonances were accomplished.

Original language	English
Pages (from-to)	91-97
Number of pages	7
Journal	FEBS Letters
Volume	212
Issue number	1
DOIs	https://doi.org/10.1016/0014-5793(87)81563-6
Publication status	Published - Feb 9 1987
Externally published	Yes

All Science Journal Classification (ASJC) codes

Biophysics
Structural Biology
Biochemistry
Molecular Biology
Genetics
Cell Biology

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10.1016/0014-5793(87)81563-6

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abstract = "We applied multiple relayed COSY and 2D homonuclear Hartman-Hahn spectroscopy to globoside, a glycolipid purified from human red blood cells. The subspectra corresponding to individual sugar components were extracted even from overlapping proton resonances by taking the cross sections of 2D spectra parallel to the F2 axis at anomeric proton resonances, so that unambiguous assignments of sugar proton resonances were accomplished.",

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AU - Kohda, D.

AU - Kodama, C.

AU - Suzuki, A.

PY - 1987/2/9

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AB - We applied multiple relayed COSY and 2D homonuclear Hartman-Hahn spectroscopy to globoside, a glycolipid purified from human red blood cells. The subspectra corresponding to individual sugar components were extracted even from overlapping proton resonances by taking the cross sections of 2D spectra parallel to the F2 axis at anomeric proton resonances, so that unambiguous assignments of sugar proton resonances were accomplished.

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Analysis of NMR spectra of sugar chains of glycolipids by multiple relayed COSY and 2D homonuclear. Hartman-Hahn spectroscopy

Abstract

All Science Journal Classification (ASJC) codes

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