Control of Morphology of Titania Film with High Apatite-forming Ability Derived from Chemical Treatments of Titanium with Hydrogen Peroxide

S. Kawasaki, K. Tsuru, S. Hayakawa, A. Osaka

Research output: Contribution to journalConference article

1 Citation (Scopus)

Abstract

We prepared titanium substrates with sub-micron scale pores and without sub-micron scale pores by means of chemical treatments with hydrogen peroxide and subsequent thermal treatments. Sub-micron scale pores were observed on the surface of the titanium substrate treated with 3 mass% H2O 2 at 90°C for 1 h(H1) by scanning electron microscopy. On the other hand, the sub-micron scale pores were not observed on the substrate treated with 3 mass% H2O2 at 90°C for 72 h(H72). The surface roughness, Ra of H1 and H72 substrates was 27 and 14 nm, respectively. Both substrates showed high in vitro apatite-forming ability in simulated body fluid (SBF of Kokubo's recipe). The apatite-forming ability of H72 substrate with low Ra value was higher than that of H1 with high Ra value.

Original languageEnglish
Pages (from-to)443-446
Number of pages4
JournalKey Engineering Materials
Volume254-256
Publication statusPublished - Jan 9 2004
EventThe Annual Meeting of the International Society for Ceramics in Medicine - Porto, Portugal
Duration: Nov 6 2003Nov 9 2003

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Apatites
Apatite
Titanium
Hydrogen peroxide
Hydrogen Peroxide
Substrates
Body fluids
titanium dioxide
Surface roughness
Heat treatment
Scanning electron microscopy

All Science Journal Classification (ASJC) codes

  • Materials Science(all)
  • Mechanics of Materials
  • Mechanical Engineering

Cite this

Control of Morphology of Titania Film with High Apatite-forming Ability Derived from Chemical Treatments of Titanium with Hydrogen Peroxide. / Kawasaki, S.; Tsuru, K.; Hayakawa, S.; Osaka, A.

In: Key Engineering Materials, Vol. 254-256, 09.01.2004, p. 443-446.

Research output: Contribution to journalConference article

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abstract = "We prepared titanium substrates with sub-micron scale pores and without sub-micron scale pores by means of chemical treatments with hydrogen peroxide and subsequent thermal treatments. Sub-micron scale pores were observed on the surface of the titanium substrate treated with 3 mass{\%} H2O 2 at 90°C for 1 h(H1) by scanning electron microscopy. On the other hand, the sub-micron scale pores were not observed on the substrate treated with 3 mass{\%} H2O2 at 90°C for 72 h(H72). The surface roughness, Ra of H1 and H72 substrates was 27 and 14 nm, respectively. Both substrates showed high in vitro apatite-forming ability in simulated body fluid (SBF of Kokubo's recipe). The apatite-forming ability of H72 substrate with low Ra value was higher than that of H1 with high Ra value.",
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AU - Kawasaki, S.

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AU - Osaka, A.

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N2 - We prepared titanium substrates with sub-micron scale pores and without sub-micron scale pores by means of chemical treatments with hydrogen peroxide and subsequent thermal treatments. Sub-micron scale pores were observed on the surface of the titanium substrate treated with 3 mass% H2O 2 at 90°C for 1 h(H1) by scanning electron microscopy. On the other hand, the sub-micron scale pores were not observed on the substrate treated with 3 mass% H2O2 at 90°C for 72 h(H72). The surface roughness, Ra of H1 and H72 substrates was 27 and 14 nm, respectively. Both substrates showed high in vitro apatite-forming ability in simulated body fluid (SBF of Kokubo's recipe). The apatite-forming ability of H72 substrate with low Ra value was higher than that of H1 with high Ra value.

AB - We prepared titanium substrates with sub-micron scale pores and without sub-micron scale pores by means of chemical treatments with hydrogen peroxide and subsequent thermal treatments. Sub-micron scale pores were observed on the surface of the titanium substrate treated with 3 mass% H2O 2 at 90°C for 1 h(H1) by scanning electron microscopy. On the other hand, the sub-micron scale pores were not observed on the substrate treated with 3 mass% H2O2 at 90°C for 72 h(H72). The surface roughness, Ra of H1 and H72 substrates was 27 and 14 nm, respectively. Both substrates showed high in vitro apatite-forming ability in simulated body fluid (SBF of Kokubo's recipe). The apatite-forming ability of H72 substrate with low Ra value was higher than that of H1 with high Ra value.

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