Crystal structure analysis of a hexatungstate by a high-energy X-ray diffraction experiment using an imaging plate Weissenberg camera at the BL04B2 beamline of SPring-81

Tomoji Ozeki, Katsuhiro Kusaka, Noritaka Honma, Yuji Nakamura, Setsuko Nakamura, Shunsuke Oike, Nobuhiro Yasuda, Hiroyuki Imura, Hidehiro Uekusa, Maiko Isshiki, Chuji Katayama, Yuji Ohashi

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Abstract

An imaging plate Weissenberg camera was installed in the BL04B2 beamline of SPring-8 aiming at automated crystal structure determinations of small molecules. Since this beamline is designed to provide X-rays with the energies higher than 37 keV (λ < 0.33 Å), this camera is advantageous in crystal structure analyses of heavily X-ray absorbing materials. The title crystal structure analysis led to precise positional parameters and well-behaved displacement parameters not only for heavy atoms but also for light atoms.

Original languageEnglish
Pages (from-to)804-805
Number of pages2
JournalChemistry Letters
Issue number8
DOIs
Publication statusPublished - Jan 1 2001
Externally publishedYes

All Science Journal Classification (ASJC) codes

  • Chemistry(all)

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    Ozeki, T., Kusaka, K., Honma, N., Nakamura, Y., Nakamura, S., Oike, S., Yasuda, N., Imura, H., Uekusa, H., Isshiki, M., Katayama, C., & Ohashi, Y. (2001). Crystal structure analysis of a hexatungstate by a high-energy X-ray diffraction experiment using an imaging plate Weissenberg camera at the BL04B2 beamline of SPring-81. Chemistry Letters, (8), 804-805. https://doi.org/10.1246/cl.2001.804