Crystal structure of N-[(6-methoxy-4-oxo-1,4-dihydroquinolin-3-yl) methyl]-2,2-dimethylpropanamide

Junzo Hirano, Kenji Hamase, Takeyuki Akita, Kiyoshi Zaitsu

Research output: Contribution to journalComment/debate

1 Citation (Scopus)

Abstract

The crystal structure of N-[(6-methoxy-4-oxo-1,4-dihydroquinolin-3-yl)methyl]-2,2-dimethylpropanamide (2) was determined by X-ray diffraction analysis. The compound crystallized in the triclinic system, space group P1, with cell parameters of a = 7.829(3)Å, b = 8.995(4)Å, c = 10.646(5)Å, α = 85.86(2)o, β = 86.99(1)o, γ = 88.00(2)o, and Z = 2. The structure was refined by full-matrix least-squares to final values of R1 = 0.049 and wR2 = 0.103. The intermolecular hydrogen bonds of the type N-H···O were observed in the structure. 2004

Original languageEnglish
JournalAnalytical Sciences: X-ray Structure Analysis Online
Volume20
Issue number3
DOIs
Publication statusPublished - Jan 1 2004

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X ray diffraction analysis
Hydrogen bonds
Crystal structure
1,4-dihydroquinoline

All Science Journal Classification (ASJC) codes

  • Analytical Chemistry
  • Materials Chemistry

Cite this

Crystal structure of N-[(6-methoxy-4-oxo-1,4-dihydroquinolin-3-yl) methyl]-2,2-dimethylpropanamide. / Hirano, Junzo; Hamase, Kenji; Akita, Takeyuki; Zaitsu, Kiyoshi.

In: Analytical Sciences: X-ray Structure Analysis Online, Vol. 20, No. 3, 01.01.2004.

Research output: Contribution to journalComment/debate

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abstract = "The crystal structure of N-[(6-methoxy-4-oxo-1,4-dihydroquinolin-3-yl)methyl]-2,2-dimethylpropanamide (2) was determined by X-ray diffraction analysis. The compound crystallized in the triclinic system, space group P1, with cell parameters of a = 7.829(3){\AA}, b = 8.995(4){\AA}, c = 10.646(5){\AA}, α = 85.86(2)o, β = 86.99(1)o, γ = 88.00(2)o, and Z = 2. The structure was refined by full-matrix least-squares to final values of R1 = 0.049 and wR2 = 0.103. The intermolecular hydrogen bonds of the type N-H···O were observed in the structure. 2004",
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AU - Zaitsu, Kiyoshi

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N2 - The crystal structure of N-[(6-methoxy-4-oxo-1,4-dihydroquinolin-3-yl)methyl]-2,2-dimethylpropanamide (2) was determined by X-ray diffraction analysis. The compound crystallized in the triclinic system, space group P1, with cell parameters of a = 7.829(3)Å, b = 8.995(4)Å, c = 10.646(5)Å, α = 85.86(2)o, β = 86.99(1)o, γ = 88.00(2)o, and Z = 2. The structure was refined by full-matrix least-squares to final values of R1 = 0.049 and wR2 = 0.103. The intermolecular hydrogen bonds of the type N-H···O were observed in the structure. 2004

AB - The crystal structure of N-[(6-methoxy-4-oxo-1,4-dihydroquinolin-3-yl)methyl]-2,2-dimethylpropanamide (2) was determined by X-ray diffraction analysis. The compound crystallized in the triclinic system, space group P1, with cell parameters of a = 7.829(3)Å, b = 8.995(4)Å, c = 10.646(5)Å, α = 85.86(2)o, β = 86.99(1)o, γ = 88.00(2)o, and Z = 2. The structure was refined by full-matrix least-squares to final values of R1 = 0.049 and wR2 = 0.103. The intermolecular hydrogen bonds of the type N-H···O were observed in the structure. 2004

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