Direct analysis of phenolic extractives in wood by thermochemolysis-gas chromatography in the presence of tetrabutylammonium hydroxide

Yasuyuki Ishida, Kuniyoshi Goto, Hiroaki Yokoi, Shin Tsuge, Hajime Ohtani, Tetsuya Sonoda, Toshihiro Ona

Research output: Contribution to journalArticle

36 Citations (Scopus)

Abstract

Thermochemolysis-gas chromatography in the presence of tetrabutylammonium hydroxide was applied to the direct determination of phenolic compounds present as "extractives" in a wood sample (Eucalyptus camaldulensis). The phenolic extractives converted into their perbutyl derivatives were separated from the other phenolic products derived from the lignin skeleton in the observed chromatogram of the wood sample. On the basis of their peak intensities, the contents of the phenolic extractives in the wood sample were rapidly and precisely determined without using preliminary solvent extraction of the wood sample.

Original languageEnglish
Pages (from-to)200-206
Number of pages7
JournalJournal of Analytical and Applied Pyrolysis
Volume78
Issue number1
DOIs
Publication statusPublished - Jan 1 2007

Fingerprint

gas chromatography
Gas chromatography
hydroxides
Wood
solvent extraction
lignin
Lignin
Solvent extraction
musculoskeletal system
Derivatives
tetrabutylammonium
products

All Science Journal Classification (ASJC) codes

  • Chemistry(all)
  • Chemical Engineering(all)

Cite this

Direct analysis of phenolic extractives in wood by thermochemolysis-gas chromatography in the presence of tetrabutylammonium hydroxide. / Ishida, Yasuyuki; Goto, Kuniyoshi; Yokoi, Hiroaki; Tsuge, Shin; Ohtani, Hajime; Sonoda, Tetsuya; Ona, Toshihiro.

In: Journal of Analytical and Applied Pyrolysis, Vol. 78, No. 1, 01.01.2007, p. 200-206.

Research output: Contribution to journalArticle

Ishida, Yasuyuki ; Goto, Kuniyoshi ; Yokoi, Hiroaki ; Tsuge, Shin ; Ohtani, Hajime ; Sonoda, Tetsuya ; Ona, Toshihiro. / Direct analysis of phenolic extractives in wood by thermochemolysis-gas chromatography in the presence of tetrabutylammonium hydroxide. In: Journal of Analytical and Applied Pyrolysis. 2007 ; Vol. 78, No. 1. pp. 200-206.
@article{ad9fbce2a2fe4de889e6a50fd2008d7a,
title = "Direct analysis of phenolic extractives in wood by thermochemolysis-gas chromatography in the presence of tetrabutylammonium hydroxide",
abstract = "Thermochemolysis-gas chromatography in the presence of tetrabutylammonium hydroxide was applied to the direct determination of phenolic compounds present as {"}extractives{"} in a wood sample (Eucalyptus camaldulensis). The phenolic extractives converted into their perbutyl derivatives were separated from the other phenolic products derived from the lignin skeleton in the observed chromatogram of the wood sample. On the basis of their peak intensities, the contents of the phenolic extractives in the wood sample were rapidly and precisely determined without using preliminary solvent extraction of the wood sample.",
author = "Yasuyuki Ishida and Kuniyoshi Goto and Hiroaki Yokoi and Shin Tsuge and Hajime Ohtani and Tetsuya Sonoda and Toshihiro Ona",
year = "2007",
month = "1",
day = "1",
doi = "10.1016/j.jaap.2006.06.009",
language = "English",
volume = "78",
pages = "200--206",
journal = "Journal of Analytical and Applied Pyrolysis",
issn = "0165-2370",
publisher = "Elsevier",
number = "1",

}

TY - JOUR

T1 - Direct analysis of phenolic extractives in wood by thermochemolysis-gas chromatography in the presence of tetrabutylammonium hydroxide

AU - Ishida, Yasuyuki

AU - Goto, Kuniyoshi

AU - Yokoi, Hiroaki

AU - Tsuge, Shin

AU - Ohtani, Hajime

AU - Sonoda, Tetsuya

AU - Ona, Toshihiro

PY - 2007/1/1

Y1 - 2007/1/1

N2 - Thermochemolysis-gas chromatography in the presence of tetrabutylammonium hydroxide was applied to the direct determination of phenolic compounds present as "extractives" in a wood sample (Eucalyptus camaldulensis). The phenolic extractives converted into their perbutyl derivatives were separated from the other phenolic products derived from the lignin skeleton in the observed chromatogram of the wood sample. On the basis of their peak intensities, the contents of the phenolic extractives in the wood sample were rapidly and precisely determined without using preliminary solvent extraction of the wood sample.

AB - Thermochemolysis-gas chromatography in the presence of tetrabutylammonium hydroxide was applied to the direct determination of phenolic compounds present as "extractives" in a wood sample (Eucalyptus camaldulensis). The phenolic extractives converted into their perbutyl derivatives were separated from the other phenolic products derived from the lignin skeleton in the observed chromatogram of the wood sample. On the basis of their peak intensities, the contents of the phenolic extractives in the wood sample were rapidly and precisely determined without using preliminary solvent extraction of the wood sample.

UR - http://www.scopus.com/inward/record.url?scp=33845291133&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=33845291133&partnerID=8YFLogxK

U2 - 10.1016/j.jaap.2006.06.009

DO - 10.1016/j.jaap.2006.06.009

M3 - Article

AN - SCOPUS:33845291133

VL - 78

SP - 200

EP - 206

JO - Journal of Analytical and Applied Pyrolysis

JF - Journal of Analytical and Applied Pyrolysis

SN - 0165-2370

IS - 1

ER -