TY - JOUR
T1 - Effects of heating rate in calcination process on microstructures of Y123 precursor and final films formed by advanced TFA-MOD method
AU - Matsuda, Junko S.
AU - Nakaoka, Koichi
AU - Tokunaga, Yoshitaka
AU - Teranishi, Ryo
AU - Koyama, Satoshi
AU - Aoki, Yuji
AU - Fuji, Hiroshi
AU - Yajima, Akiraasa
AU - Yamada, Yutaka
AU - Izumi, Teruo
AU - Shiohara, Yuh
N1 - Funding Information:
Manuscript received October 5, 2004. This work was supported by the New Energy and Industrial Technology Development Organization (NEDO) as Collaborative Research and Development of Fundamental Technologies for Superconductivity Applications.
Copyright:
Copyright 2008 Elsevier B.V., All rights reserved.
PY - 2005/6
Y1 - 2005/6
N2 - We have investigated the effects of heating rates in the calcination process on microstructures of Y123 precursor and final films. As a result, it was found that there is CuO segregation in the vicinity of the Y123 precursor film surface, when the precursor is prepared at a rapid heating rate in the calcination. In the case of heat-treating this precursor film in the crystallization process, many large pores and misoriented Y123 crystals tend to remain in the Y123 final film. It is important to control the heating rate in the calcination, in order to attain higher Jc of the Y123 final films.
AB - We have investigated the effects of heating rates in the calcination process on microstructures of Y123 precursor and final films. As a result, it was found that there is CuO segregation in the vicinity of the Y123 precursor film surface, when the precursor is prepared at a rapid heating rate in the calcination. In the case of heat-treating this precursor film in the crystallization process, many large pores and misoriented Y123 crystals tend to remain in the Y123 final film. It is important to control the heating rate in the calcination, in order to attain higher Jc of the Y123 final films.
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U2 - 10.1109/TASC.2005.847759
DO - 10.1109/TASC.2005.847759
M3 - Article
AN - SCOPUS:22144497744
SN - 1051-8223
VL - 15
SP - 2652
EP - 2655
JO - IEEE Transactions on Applied Superconductivity
JF - IEEE Transactions on Applied Superconductivity
IS - 2 PART III
ER -