Evaluation of local creep strain in face-centred cubic heatresistant alloys using electron backscattered diffraction analysis

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Abstract

Creep strain in SUS347HTB austenitic heat-resistant steel and Ni-based heat-resistant alloys was evaluated by electron backscattered diffraction (EBSD). Localized crystallographic misorientations in the crept samples were quantified by using misorientation indicators such as kernel average misorientation and grain reference orientation deviation. In most crept samples, the misorientation indicators increased with creep deformation. However, this trend was not observed for alloys with dense dispersions. We proposed a method to extract and evaluate data only near the grain boundary from the total EBSD data. For Ni-based alloys, the misorientation indicators tended to increase preferentially near grain boundaries. Conversely, there was no substantial difference between the misorientation indicators near grain boundaries and the intergranular region for SUS347HTB. Consequently, although it is necessary to limit the region for evaluating the misorientation indicators according to the dispersion density of the reinforcing phase in the materials, the misorientation indicators, such as kernel average misorientation or grain reference orientation deviation, are useful for evaluating the creep strain in face-centred cubic heat-resistant alloys.

Original languageEnglish
Pages (from-to)851-856
Number of pages6
Journalisij international
Volume57
Issue number5
DOIs
Publication statusPublished - Jan 1 2017

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Electron diffraction
Creep
Grain boundaries
Superalloys
Steel
Dispersions

All Science Journal Classification (ASJC) codes

  • Mechanics of Materials
  • Mechanical Engineering
  • Metals and Alloys
  • Materials Chemistry

Cite this

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title = "Evaluation of local creep strain in face-centred cubic heatresistant alloys using electron backscattered diffraction analysis",
abstract = "Creep strain in SUS347HTB austenitic heat-resistant steel and Ni-based heat-resistant alloys was evaluated by electron backscattered diffraction (EBSD). Localized crystallographic misorientations in the crept samples were quantified by using misorientation indicators such as kernel average misorientation and grain reference orientation deviation. In most crept samples, the misorientation indicators increased with creep deformation. However, this trend was not observed for alloys with dense dispersions. We proposed a method to extract and evaluate data only near the grain boundary from the total EBSD data. For Ni-based alloys, the misorientation indicators tended to increase preferentially near grain boundaries. Conversely, there was no substantial difference between the misorientation indicators near grain boundaries and the intergranular region for SUS347HTB. Consequently, although it is necessary to limit the region for evaluating the misorientation indicators according to the dispersion density of the reinforcing phase in the materials, the misorientation indicators, such as kernel average misorientation or grain reference orientation deviation, are useful for evaluating the creep strain in face-centred cubic heat-resistant alloys.",
author = "Shigeto Yamasaki and Masatoshi Mitsuhara and Hideharu Nakashima and Mitsuharu Yonemura",
year = "2017",
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T1 - Evaluation of local creep strain in face-centred cubic heatresistant alloys using electron backscattered diffraction analysis

AU - Yamasaki, Shigeto

AU - Mitsuhara, Masatoshi

AU - Nakashima, Hideharu

AU - Yonemura, Mitsuharu

PY - 2017/1/1

Y1 - 2017/1/1

N2 - Creep strain in SUS347HTB austenitic heat-resistant steel and Ni-based heat-resistant alloys was evaluated by electron backscattered diffraction (EBSD). Localized crystallographic misorientations in the crept samples were quantified by using misorientation indicators such as kernel average misorientation and grain reference orientation deviation. In most crept samples, the misorientation indicators increased with creep deformation. However, this trend was not observed for alloys with dense dispersions. We proposed a method to extract and evaluate data only near the grain boundary from the total EBSD data. For Ni-based alloys, the misorientation indicators tended to increase preferentially near grain boundaries. Conversely, there was no substantial difference between the misorientation indicators near grain boundaries and the intergranular region for SUS347HTB. Consequently, although it is necessary to limit the region for evaluating the misorientation indicators according to the dispersion density of the reinforcing phase in the materials, the misorientation indicators, such as kernel average misorientation or grain reference orientation deviation, are useful for evaluating the creep strain in face-centred cubic heat-resistant alloys.

AB - Creep strain in SUS347HTB austenitic heat-resistant steel and Ni-based heat-resistant alloys was evaluated by electron backscattered diffraction (EBSD). Localized crystallographic misorientations in the crept samples were quantified by using misorientation indicators such as kernel average misorientation and grain reference orientation deviation. In most crept samples, the misorientation indicators increased with creep deformation. However, this trend was not observed for alloys with dense dispersions. We proposed a method to extract and evaluate data only near the grain boundary from the total EBSD data. For Ni-based alloys, the misorientation indicators tended to increase preferentially near grain boundaries. Conversely, there was no substantial difference between the misorientation indicators near grain boundaries and the intergranular region for SUS347HTB. Consequently, although it is necessary to limit the region for evaluating the misorientation indicators according to the dispersion density of the reinforcing phase in the materials, the misorientation indicators, such as kernel average misorientation or grain reference orientation deviation, are useful for evaluating the creep strain in face-centred cubic heat-resistant alloys.

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