Fabrication and some mechanical properties of SiC whisker-reinforced Si3N4 composites utilizing underwater-shock pressure

Ryuichi Tomoshige, Akira Chiba, Minoru Nishida, Kihachiro Imamura, Shigeru Itoh, Masahiro Fujita

Research output: Contribution to journalArticle

Abstract

SiC whisker-reinforced Si3N4-based composites without additives were compacted by underwater-shock wave. The composites contained 10, 20 and 30 vol% SiC whisker as reinforcements. There were no macrocracks in all shock compacted composites. The as-compacted and specimens sintered at various temperatures for 5h were characterized by the measurements of relative density, micro Vickers hardness and fracture toughness. The relative density of a sintered Si3N4-10 vol% SiC whisker composite was higher than that of sintered Si3N4-20 and 30 vol% SiC whisker composites, and reached the theoretical density by sintering at 1973 K. Hardness of each composite increased up to 1823 K in proportion to sintering temperature, and then saturated above 1823 K. The hardness and fracture toughness of the Si3N4-30 vol% SiC whisker composite sintered at 1973 K were about 29 GPa and 5.0 MPa√m, respectively. The fracture toughness was 25% higher than those of monolithic Si3N4 and other obtained composites sintered at the same temperature. SEM observation showed that whisker bridging and deflection were observed in sintered composites and that the matrix of the Si3N4-30 vol% SiC whisker composite consisted of plate-like and submicron order fine needle-like β-Si3N4 grains.

Original languageEnglish
Pages (from-to)445-450
Number of pages6
JournalNippon Seramikkusu Kyokai Gakujutsu Ronbunshi/Journal of the Ceramic Society of Japan
Volume101
Issue number1172
DOIs
Publication statusPublished - Jan 1 1993
Externally publishedYes

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whisker composites
shock
mechanical properties
Fabrication
Mechanical properties
fabrication
composite materials
Composite materials
fracture strength
toughness
sintering
hardness
Fracture toughness
Vickers hardness
reinforcement
needles
Sintering
Hardness
temperature
silicon nitride

All Science Journal Classification (ASJC) codes

  • Ceramics and Composites
  • Chemistry(all)
  • Condensed Matter Physics
  • Materials Chemistry

Cite this

Fabrication and some mechanical properties of SiC whisker-reinforced Si3N4 composites utilizing underwater-shock pressure. / Tomoshige, Ryuichi; Chiba, Akira; Nishida, Minoru; Imamura, Kihachiro; Itoh, Shigeru; Fujita, Masahiro.

In: Nippon Seramikkusu Kyokai Gakujutsu Ronbunshi/Journal of the Ceramic Society of Japan, Vol. 101, No. 1172, 01.01.1993, p. 445-450.

Research output: Contribution to journalArticle

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abstract = "SiC whisker-reinforced Si3N4-based composites without additives were compacted by underwater-shock wave. The composites contained 10, 20 and 30 vol{\%} SiC whisker as reinforcements. There were no macrocracks in all shock compacted composites. The as-compacted and specimens sintered at various temperatures for 5h were characterized by the measurements of relative density, micro Vickers hardness and fracture toughness. The relative density of a sintered Si3N4-10 vol{\%} SiC whisker composite was higher than that of sintered Si3N4-20 and 30 vol{\%} SiC whisker composites, and reached the theoretical density by sintering at 1973 K. Hardness of each composite increased up to 1823 K in proportion to sintering temperature, and then saturated above 1823 K. The hardness and fracture toughness of the Si3N4-30 vol{\%} SiC whisker composite sintered at 1973 K were about 29 GPa and 5.0 MPa√m, respectively. The fracture toughness was 25{\%} higher than those of monolithic Si3N4 and other obtained composites sintered at the same temperature. SEM observation showed that whisker bridging and deflection were observed in sintered composites and that the matrix of the Si3N4-30 vol{\%} SiC whisker composite consisted of plate-like and submicron order fine needle-like β-Si3N4 grains.",
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