Fracture behavior and fracture toughness of pitch-based carbon fiber with an artificial notch introduced by a focused ion beam

Shojiro Ochiai, Shigetaka Kuboshima, Hiroshi Okuda, Kohei Morishita, Eiki Tsushima

Research output: Contribution to journalArticlepeer-review

5 Citations (Scopus)

Abstract

Fracture behavior and fracture toughness of pitch-based carbon fiber were studied using the fiber specimens into which an artificial mode I type straight-fronted edge notch was introduced by a focused-ion (Ga +)-beam. Two fiber samples were used for experiment. One was the as-supplied pitch-based fiber (GRANOC XN-35®, Nippon Graphite Fiber Corporation) and another was the same fiber heat-treated at 3273 K for 3.6 × 103 s in argon atmosphere. The heat-treatment raised the Youngs modulus from 370 to 840 GPa. The fracture toughness value of the as-supplied fiber was ~1.4 MPa m1/2 and the apparent fracture toughness value of the heat-treated fiber was ~4.2 MPa m1/2, which were estimated from the measured values of the strength (σf), notch depth (a), and fiber diameter (D) and correction factor. The increase in the apparent fracture toughness value due to the heat-treatment was attributed to the enhanced c-plane array and its cleavage fracture in longitudinal direction ahead of the notch tip. The analysis of the fracture strength - notch depth relation showed that the fracture of the as-supplied fiber obeys the fracture mechanical criterion and the fracture of the heat-treated fiber obeys the net stress criterion.

Original languageEnglish
Pages (from-to)265-279
Number of pages15
JournalComposite Interfaces
Volume21
Issue number4
DOIs
Publication statusPublished - May 4 2014
Externally publishedYes

All Science Journal Classification (ASJC) codes

  • Ceramics and Composites
  • Physics and Astronomy(all)
  • Surfaces, Coatings and Films

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