Lithium niobium disulfide, Li0.63NbS2, has been prepared by a metathesis reaction between physically separated solid reactants, i.e. separated reactant metathesis (SRM). Single-crystal data were collected at reduced temperature [150 (2) K], yielding a refined Li content of y = 0.63 (6). The Li content in the crystalline samples was also determined analytically by flame photometry. The compound crystallizes in hexagonal space group P63/mmc (No. 194), with Li+ ions situated in octahedral sites between NbS2 layers.
|Journal||Acta Crystallographica Section C: Crystal Structure Communications|
|Publication status||Published - Jan 1 2003|
All Science Journal Classification (ASJC) codes
- Biochemistry, Genetics and Molecular Biology(all)