Measurement of viscosity of multi-component glasses in the wide range for fiber drawing

Shigeru Fujino, Hideyuki Ijiri, Fumiyuki Shimizu, Kenji Morinaga

Research output: Contribution to journalArticle

26 Citations (Scopus)

Abstract

The viscosity-temperature behavior in the wide range 10-2∼1012Pa·s were presented for various glass systems: oxide, fluoride, halide, and chalcogenide. There is no single technique that can be utilized to measure the viscosity of glass over the entire range, spaning roughly 14 orders of magnitude. The viscosity was measured by a penetration viscometry method at low-temperature viscosity region (107∼1012 Pa·s) and by a rotational viscometry method at high-temperature viscosity region (10-2∼101 Pa·s). It was found the viscosity can be expressed by the Cohen-Grest equation over a wide temperature. The working point, Tw(103 Pa·s), the softening point, Ts(106.65 Pa·s) and the working range-temperature interval between the Tw and the Ts were determined using the measured viscosity data and the viscosity-temperature equation. We discussed the technical term of fiber drawing from the viewpoint of viscosity-temperature behavior and thermal stability of glass crystalized as a function of heat treatment time, tD at the drawing temperature. The results indicate that silica and lead silicate glasses are prefered for fiber drawing.

Original languageEnglish
Pages (from-to)106-110
Number of pages5
JournalNippon Kinzoku Gakkaishi/Journal of the Japan Institute of Metals
Volume62
Issue number1
DOIs
Publication statusPublished - 1998

Fingerprint

Viscosity
viscosity
Glass
fibers
Fibers
glass
viscometry
Temperature
Viscosity measurement
temperature
Fluorides
Silicon Dioxide
softening
Oxides
Silicates
halides
fluorides
silicates
Thermodynamic stability
heat treatment

All Science Journal Classification (ASJC) codes

  • Condensed Matter Physics
  • Mechanics of Materials
  • Metals and Alloys
  • Materials Chemistry

Cite this

Measurement of viscosity of multi-component glasses in the wide range for fiber drawing. / Fujino, Shigeru; Ijiri, Hideyuki; Shimizu, Fumiyuki; Morinaga, Kenji.

In: Nippon Kinzoku Gakkaishi/Journal of the Japan Institute of Metals, Vol. 62, No. 1, 1998, p. 106-110.

Research output: Contribution to journalArticle

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