Observation of precipitates in aluminum alloys by sub-micrometer resolution tomography using fresnel zone plate

Hiroyuki Toda, Keisuke Minami, Masakazu Kobayashi, Kentaro Uesugi, Akihisa Takeuchi, Toshiro Kobayashi

Research output: Chapter in Book/Report/Conference proceedingConference contribution

3 Citations (Scopus)

Abstract

An X-ray microtomography combined with hard X-ray imaging microscopy, that potentially has a spatial resolution of the order of 10 to 100 nm, has been applied to the three-dimensional observation of internal microstructural features in overaged Al-Ag alloys. A Fresnel zone plate is used as an objective with a magnification of 49.3 times. Imaging of resolution test patterns has indicated spatial resolutions of around 180 and 200 nm in the vertical and horizontal directions, respectively. This paper reports the first impression of the microstructural imaging by means of such a high-resolution imaging microtomography. Precipitate microstructures are readily observed and quantified in terms of volume fraction and orientation. Conventional microtomography with a simple projection geometry is also applied for comparison purpose at the highest resolution level currently available at a third generation synchrotron facility. It would appear that the present technique provides a unique potential to observe the 3-D geometry and spatial distribution of nanoscopic features inside samples that are several orders of magnitude thicker than thin-foil specimens for TEM observation.

Original languageEnglish
Title of host publicationAluminium Alloys 2006
Subtitle of host publicationResearch Through Innovation and Technology - Proceedings of the 10th International Conference on Aluminium Alloys
Pages1361-1366
Number of pages6
EditionPART 2
Publication statusPublished - Dec 1 2006
Externally publishedYes
Event10th International Conference on Aluminium Alloys, (ICAA-10) - Vancouver, Canada
Duration: Jul 9 2006Jul 13 2006

Publication series

NameMaterials Science Forum
NumberPART 2
Volume519-521
ISSN (Print)0255-5476

Other

Other10th International Conference on Aluminium Alloys, (ICAA-10)
CountryCanada
CityVancouver
Period7/9/067/13/06

Fingerprint

aluminum alloys
Tomography
micrometers
Precipitates
precipitates
Aluminum alloys
tomography
spatial resolution
Imaging techniques
high resolution
geometry
magnification
foils
spatial distribution
synchrotrons
x rays
projection
microscopy
X rays
transmission electron microscopy

All Science Journal Classification (ASJC) codes

  • Materials Science(all)
  • Condensed Matter Physics
  • Mechanics of Materials
  • Mechanical Engineering

Cite this

Toda, H., Minami, K., Kobayashi, M., Uesugi, K., Takeuchi, A., & Kobayashi, T. (2006). Observation of precipitates in aluminum alloys by sub-micrometer resolution tomography using fresnel zone plate. In Aluminium Alloys 2006: Research Through Innovation and Technology - Proceedings of the 10th International Conference on Aluminium Alloys (PART 2 ed., pp. 1361-1366). (Materials Science Forum; Vol. 519-521, No. PART 2).

Observation of precipitates in aluminum alloys by sub-micrometer resolution tomography using fresnel zone plate. / Toda, Hiroyuki; Minami, Keisuke; Kobayashi, Masakazu; Uesugi, Kentaro; Takeuchi, Akihisa; Kobayashi, Toshiro.

Aluminium Alloys 2006: Research Through Innovation and Technology - Proceedings of the 10th International Conference on Aluminium Alloys. PART 2. ed. 2006. p. 1361-1366 (Materials Science Forum; Vol. 519-521, No. PART 2).

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Toda, H, Minami, K, Kobayashi, M, Uesugi, K, Takeuchi, A & Kobayashi, T 2006, Observation of precipitates in aluminum alloys by sub-micrometer resolution tomography using fresnel zone plate. in Aluminium Alloys 2006: Research Through Innovation and Technology - Proceedings of the 10th International Conference on Aluminium Alloys. PART 2 edn, Materials Science Forum, no. PART 2, vol. 519-521, pp. 1361-1366, 10th International Conference on Aluminium Alloys, (ICAA-10), Vancouver, Canada, 7/9/06.
Toda H, Minami K, Kobayashi M, Uesugi K, Takeuchi A, Kobayashi T. Observation of precipitates in aluminum alloys by sub-micrometer resolution tomography using fresnel zone plate. In Aluminium Alloys 2006: Research Through Innovation and Technology - Proceedings of the 10th International Conference on Aluminium Alloys. PART 2 ed. 2006. p. 1361-1366. (Materials Science Forum; PART 2).
Toda, Hiroyuki ; Minami, Keisuke ; Kobayashi, Masakazu ; Uesugi, Kentaro ; Takeuchi, Akihisa ; Kobayashi, Toshiro. / Observation of precipitates in aluminum alloys by sub-micrometer resolution tomography using fresnel zone plate. Aluminium Alloys 2006: Research Through Innovation and Technology - Proceedings of the 10th International Conference on Aluminium Alloys. PART 2. ed. 2006. pp. 1361-1366 (Materials Science Forum; PART 2).
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