Spectroscopic evaluation of nanocomposite formation from amorphous complex compound in Si3N4-BN system

Junichi Hojo, Koji Eto, Masato Uehara, Naoya Enomoto

Research output: Contribution to journalArticle

4 Citations (Scopus)

Abstract

The phase separation behavior of amorphous Si3N4-BN composite powder was investigated by spectroscopic methods. The powder was heat-treated in N2 at 1200-1600°C with and without Y2O3-Al2O3 sintering aid. The IR analysis indicated that Si3N4 and BN were separated above 1400°C and the crystallization was accelerated by the sintering aid. It was found from the XPS analysis that BN was expelled from the inside to the surface of composite particles during heating. Finally; The dense nanocomposite of Si3N4-BN system was obtained by hot pressing at 1800°C.

Original languageEnglish
Pages (from-to)2169-2172
Number of pages4
JournalScripta Materialia
Volume44
Issue number8-9
DOIs
Publication statusPublished - May 18 2001

Fingerprint

complex compounds
Nanocomposites
nanocomposites
sintering
Sintering
Powders
composite materials
hot pressing
evaluation
Composite materials
Hot pressing
Phase separation
X ray photoelectron spectroscopy
Crystallization
crystallization
Heating
heat
heating
silicon nitride
Hot Temperature

All Science Journal Classification (ASJC) codes

  • Materials Science(all)
  • Condensed Matter Physics

Cite this

Spectroscopic evaluation of nanocomposite formation from amorphous complex compound in Si3N4-BN system. / Hojo, Junichi; Eto, Koji; Uehara, Masato; Enomoto, Naoya.

In: Scripta Materialia, Vol. 44, No. 8-9, 18.05.2001, p. 2169-2172.

Research output: Contribution to journalArticle

Hojo, Junichi ; Eto, Koji ; Uehara, Masato ; Enomoto, Naoya. / Spectroscopic evaluation of nanocomposite formation from amorphous complex compound in Si3N4-BN system. In: Scripta Materialia. 2001 ; Vol. 44, No. 8-9. pp. 2169-2172.
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