Study on the nature of the electrochemically synthesized hard Fe-15.4 mass% Ni-0.70 mass% C alloy film

A. S.M.A. Haseeb, Y. Hayashi, M. Masuda, Makoto Arita

Research output: Contribution to journalArticle

Abstract

Electrochemical synthesis of hard Fe-15.4 mass% Ni-0.70 mass% C alloy film with a hardness 750 HV was carried out from sulfate-based bath containing a small amount of citric acid and L-ascorbic acid. The nature of the alloy was investigated by different characterization techniques including x-ray diffraction, x-ray photoelectron spectroscopy, scanning electron microscopy, transmission electron microscopy, Mössbauer spectroscopy, differential scanning calorimetry, and magnetic measurements. The decomposition behavior of the alloy was also studied and compared with that of thermally prepared martensite. It was found that the electrochemically deposited Fe-Ni-C alloy exists in a state that is ahead of the freshly quenched state of martensite. It is suggested that the state of the electrochemically deposited Fe-15.4 mass% Ni-0.70 mass% C alloy corresponds to the state of thermal martensite, which had been heated to the preprecipitation stage of tempering.

Original languageEnglish
Pages (from-to)840-847
Number of pages8
JournalJournal of Materials Research
Volume18
Issue number4
DOIs
Publication statusPublished - Jan 1 2003

Fingerprint

martensite
Martensite
X rays
electrochemical synthesis
tempering
ascorbic acid
citric acid
Ascorbic acid
Citric acid
Magnetic variables measurement
Tempering
Photoelectron spectroscopy
Citric Acid
x ray spectroscopy
Ascorbic Acid
Sulfates
magnetic measurement
Differential scanning calorimetry
baths
sulfates

All Science Journal Classification (ASJC) codes

  • Materials Science(all)
  • Condensed Matter Physics
  • Mechanics of Materials
  • Mechanical Engineering

Cite this

Study on the nature of the electrochemically synthesized hard Fe-15.4 mass% Ni-0.70 mass% C alloy film. / Haseeb, A. S.M.A.; Hayashi, Y.; Masuda, M.; Arita, Makoto.

In: Journal of Materials Research, Vol. 18, No. 4, 01.01.2003, p. 840-847.

Research output: Contribution to journalArticle

@article{01ecbe150d6f4e3bb05a2e4649f21dbd,
title = "Study on the nature of the electrochemically synthesized hard Fe-15.4 mass{\%} Ni-0.70 mass{\%} C alloy film",
abstract = "Electrochemical synthesis of hard Fe-15.4 mass{\%} Ni-0.70 mass{\%} C alloy film with a hardness 750 HV was carried out from sulfate-based bath containing a small amount of citric acid and L-ascorbic acid. The nature of the alloy was investigated by different characterization techniques including x-ray diffraction, x-ray photoelectron spectroscopy, scanning electron microscopy, transmission electron microscopy, M{\"o}ssbauer spectroscopy, differential scanning calorimetry, and magnetic measurements. The decomposition behavior of the alloy was also studied and compared with that of thermally prepared martensite. It was found that the electrochemically deposited Fe-Ni-C alloy exists in a state that is ahead of the freshly quenched state of martensite. It is suggested that the state of the electrochemically deposited Fe-15.4 mass{\%} Ni-0.70 mass{\%} C alloy corresponds to the state of thermal martensite, which had been heated to the preprecipitation stage of tempering.",
author = "Haseeb, {A. S.M.A.} and Y. Hayashi and M. Masuda and Makoto Arita",
year = "2003",
month = "1",
day = "1",
doi = "10.1557/JMR.2003.0115",
language = "English",
volume = "18",
pages = "840--847",
journal = "Journal of Materials Research",
issn = "0884-2914",
publisher = "Materials Research Society",
number = "4",

}

TY - JOUR

T1 - Study on the nature of the electrochemically synthesized hard Fe-15.4 mass% Ni-0.70 mass% C alloy film

AU - Haseeb, A. S.M.A.

AU - Hayashi, Y.

AU - Masuda, M.

AU - Arita, Makoto

PY - 2003/1/1

Y1 - 2003/1/1

N2 - Electrochemical synthesis of hard Fe-15.4 mass% Ni-0.70 mass% C alloy film with a hardness 750 HV was carried out from sulfate-based bath containing a small amount of citric acid and L-ascorbic acid. The nature of the alloy was investigated by different characterization techniques including x-ray diffraction, x-ray photoelectron spectroscopy, scanning electron microscopy, transmission electron microscopy, Mössbauer spectroscopy, differential scanning calorimetry, and magnetic measurements. The decomposition behavior of the alloy was also studied and compared with that of thermally prepared martensite. It was found that the electrochemically deposited Fe-Ni-C alloy exists in a state that is ahead of the freshly quenched state of martensite. It is suggested that the state of the electrochemically deposited Fe-15.4 mass% Ni-0.70 mass% C alloy corresponds to the state of thermal martensite, which had been heated to the preprecipitation stage of tempering.

AB - Electrochemical synthesis of hard Fe-15.4 mass% Ni-0.70 mass% C alloy film with a hardness 750 HV was carried out from sulfate-based bath containing a small amount of citric acid and L-ascorbic acid. The nature of the alloy was investigated by different characterization techniques including x-ray diffraction, x-ray photoelectron spectroscopy, scanning electron microscopy, transmission electron microscopy, Mössbauer spectroscopy, differential scanning calorimetry, and magnetic measurements. The decomposition behavior of the alloy was also studied and compared with that of thermally prepared martensite. It was found that the electrochemically deposited Fe-Ni-C alloy exists in a state that is ahead of the freshly quenched state of martensite. It is suggested that the state of the electrochemically deposited Fe-15.4 mass% Ni-0.70 mass% C alloy corresponds to the state of thermal martensite, which had been heated to the preprecipitation stage of tempering.

UR - http://www.scopus.com/inward/record.url?scp=0038337888&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=0038337888&partnerID=8YFLogxK

U2 - 10.1557/JMR.2003.0115

DO - 10.1557/JMR.2003.0115

M3 - Article

AN - SCOPUS:0038337888

VL - 18

SP - 840

EP - 847

JO - Journal of Materials Research

JF - Journal of Materials Research

SN - 0884-2914

IS - 4

ER -