Synthesis and Rietveld analysis for CoSb3 compounds prepared by Sb self-flux method

Takeshi Souma, Michitaka Ohtaki

    Research output: Chapter in Book/Report/Conference proceedingConference contribution

    2 Citations (Scopus)

    Abstract

    High purity CoSb3 bulk crystals have been successfully synthesized by Sb self-flux method and a relation between reaction conditions and chemical composition on the method has been systematically analyzed by powder XRD study using the Rietveld analysis. Sb self flux method at 923 K using 100 mesh Co elements can directly provide a single phase CoSb3 bulk crystal in a brief time of 10 h. Advantages of Sb self-flux methods will be discussed compared with other preparation methods.

    Original languageEnglish
    Title of host publicationProceedings - ICT'05
    Subtitle of host publication24th International Conference on Thermoelectrics
    Pages121-124
    Number of pages4
    DOIs
    Publication statusPublished - 2005
    EventICT'05: 24th International Conference on Thermoelectrics - Clemson, SC, United States
    Duration: Jun 19 2005Jun 23 2005

    Publication series

    NameInternational Conference on Thermoelectrics, ICT, Proceedings
    Volume2005

    Other

    OtherICT'05: 24th International Conference on Thermoelectrics
    CountryUnited States
    CityClemson, SC
    Period6/19/056/23/05

    All Science Journal Classification (ASJC) codes

    • Engineering(all)

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  • Cite this

    Souma, T., & Ohtaki, M. (2005). Synthesis and Rietveld analysis for CoSb3 compounds prepared by Sb self-flux method. In Proceedings - ICT'05: 24th International Conference on Thermoelectrics (pp. 121-124). [1519903] (International Conference on Thermoelectrics, ICT, Proceedings; Vol. 2005). https://doi.org/10.1109/ICT.2005.1519903