TY - JOUR
T1 - Synthesis of Dibromo[33]paracyclophanes
AU - Shibahara, Masahiko
AU - Watanabe, Motonori
AU - Miyazaki, Takaaki
AU - Goto, Kenta
AU - Matsumoto, Taisuke
AU - Shinmyozu, Teruo
N1 - Funding Information:
This work was partially supported by a Grant-in-Aid for Science Research (C 25410050) from the Japan Society for the Promotion of Science (JSPS), Japan, and was performed under the Cooperative Research Program of the Network Joint Research Center for Materials and Devices (IMCE, Kyushu University). M.W. thanks the World Premier International Research Center Initiative (WPI), Ministry of Education, Culture, Sports, Science and Technology of Japan (MEXT), Japan.
Publisher Copyright:
© Georg Thieme Verlag Stuttgart.
PY - 2016/3/2
Y1 - 2016/3/2
N2 - All possible pseudogeminal-, pseudoortho-, pseudometa-, and pseudopara-dibromo[3.3]paracyclophanes were synthesized by the (p-tolylsulfonyl)methyl isocyanide (TosMIC) coupling method, and characterized by the aromatic proton signals of the 1H NMR spectra and finally by the X-ray crystal structure analyses of the pseudogeminal, pseudo-?ortho, and pseudopara isomers.
AB - All possible pseudogeminal-, pseudoortho-, pseudometa-, and pseudopara-dibromo[3.3]paracyclophanes were synthesized by the (p-tolylsulfonyl)methyl isocyanide (TosMIC) coupling method, and characterized by the aromatic proton signals of the 1H NMR spectra and finally by the X-ray crystal structure analyses of the pseudogeminal, pseudo-?ortho, and pseudopara isomers.
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U2 - 10.1055/s-0035-1560421
DO - 10.1055/s-0035-1560421
M3 - Article
AN - SCOPUS:84960157759
SN - 0039-7881
VL - 48
SP - 1197
EP - 1201
JO - Synthesis
JF - Synthesis
IS - 8
ER -