Synthesis of Dibromo[33]paracyclophanes

Masahiko Shibahara, Motonori Watanabe, Takaaki Miyazaki, Kenta Goto, Taisuke Matsumoto, Teruo Shinmyozu

Research output: Contribution to journalArticle

2 Citations (Scopus)

Abstract

All possible pseudogeminal-, pseudoortho-, pseudometa-, and pseudopara-dibromo[3.3]paracyclophanes were synthesized by the (p-tolylsulfonyl)methyl isocyanide (TosMIC) coupling method, and characterized by the aromatic proton signals of the 1H NMR spectra and finally by the X-ray crystal structure analyses of the pseudogeminal, pseudo-?ortho, and pseudopara isomers.

Original languageEnglish
Pages (from-to)1197-1201
Number of pages5
JournalSynthesis (Germany)
Volume48
Issue number8
DOIs
Publication statusPublished - Mar 2 2016

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Isomers
Protons
Crystal structure
Nuclear magnetic resonance
X rays
(2.2)paracyclophane
methylisonitrile

All Science Journal Classification (ASJC) codes

  • Catalysis
  • Organic Chemistry

Cite this

Synthesis of Dibromo[33]paracyclophanes. / Shibahara, Masahiko; Watanabe, Motonori; Miyazaki, Takaaki; Goto, Kenta; Matsumoto, Taisuke; Shinmyozu, Teruo.

In: Synthesis (Germany), Vol. 48, No. 8, 02.03.2016, p. 1197-1201.

Research output: Contribution to journalArticle

Shibahara, Masahiko ; Watanabe, Motonori ; Miyazaki, Takaaki ; Goto, Kenta ; Matsumoto, Taisuke ; Shinmyozu, Teruo. / Synthesis of Dibromo[33]paracyclophanes. In: Synthesis (Germany). 2016 ; Vol. 48, No. 8. pp. 1197-1201.
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