Abstract
Rutile TiO2 with high specific surface area was synthesized by self-hydrolysis of TiOCl2 in the presence of sodium dodecyl sulfate (SDS). The aggregates of rutile acicular particles formed from 0.5 M TiOCl 2 at 50°C. In order to synthesize rutile with high specific surface area, the effect of surfactant was investigated. Three kinds of surfactants were used in this study, such as stearyltrimethylammmonium chloride (C18TAC) as cationic surfactant, polyoxyethylene lauryl ether (Brij3(5) as nonionic surfactant, and SDS as anionic surfactant. Neither C18TAC nor Brij35 was influenced on the morphology of rutile particles. On the other hand, the addition of SDS was effective for the formation of mesopore, which led to specific surface area of 210 m2/g in product.
| Original language | English |
|---|---|
| Pages (from-to) | 819-822 |
| Number of pages | 4 |
| Journal | Journal of the Ceramic Society of Japan |
| Volume | 117 |
| Issue number | 1367 |
| DOIs | |
| Publication status | Published - Jan 1 2009 |
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All Science Journal Classification (ASJC) codes
- Ceramics and Composites
- Chemistry(all)
- Condensed Matter Physics
- Materials Chemistry
Cite this
Synthesis of rutile TiO2 with high specific surface area by self-hydrolysis of TiOCl2 in the presence of SDS. / Inada, Miki; Mizue, Kei; Enomoto, Naoya; Hojo, Junichi.
In: Journal of the Ceramic Society of Japan, Vol. 117, No. 1367, 01.01.2009, p. 819-822.Research output: Contribution to journal › Article
}
TY - JOUR
T1 - Synthesis of rutile TiO2 with high specific surface area by self-hydrolysis of TiOCl2 in the presence of SDS
AU - Inada, Miki
AU - Mizue, Kei
AU - Enomoto, Naoya
AU - Hojo, Junichi
PY - 2009/1/1
Y1 - 2009/1/1
N2 - Rutile TiO2 with high specific surface area was synthesized by self-hydrolysis of TiOCl2 in the presence of sodium dodecyl sulfate (SDS). The aggregates of rutile acicular particles formed from 0.5 M TiOCl 2 at 50°C. In order to synthesize rutile with high specific surface area, the effect of surfactant was investigated. Three kinds of surfactants were used in this study, such as stearyltrimethylammmonium chloride (C18TAC) as cationic surfactant, polyoxyethylene lauryl ether (Brij3(5) as nonionic surfactant, and SDS as anionic surfactant. Neither C18TAC nor Brij35 was influenced on the morphology of rutile particles. On the other hand, the addition of SDS was effective for the formation of mesopore, which led to specific surface area of 210 m2/g in product.
AB - Rutile TiO2 with high specific surface area was synthesized by self-hydrolysis of TiOCl2 in the presence of sodium dodecyl sulfate (SDS). The aggregates of rutile acicular particles formed from 0.5 M TiOCl 2 at 50°C. In order to synthesize rutile with high specific surface area, the effect of surfactant was investigated. Three kinds of surfactants were used in this study, such as stearyltrimethylammmonium chloride (C18TAC) as cationic surfactant, polyoxyethylene lauryl ether (Brij3(5) as nonionic surfactant, and SDS as anionic surfactant. Neither C18TAC nor Brij35 was influenced on the morphology of rutile particles. On the other hand, the addition of SDS was effective for the formation of mesopore, which led to specific surface area of 210 m2/g in product.
UR - http://www.scopus.com/inward/record.url?scp=67650802511&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=67650802511&partnerID=8YFLogxK
U2 - 10.2109/jcersj2.117.819
DO - 10.2109/jcersj2.117.819
M3 - Article
AN - SCOPUS:67650802511
VL - 117
SP - 819
EP - 822
JO - Nippon Seramikkusu Kyokai Gakujutsu Ronbunshi/Journal of the Ceramic Society of Japan
JF - Nippon Seramikkusu Kyokai Gakujutsu Ronbunshi/Journal of the Ceramic Society of Japan
SN - 1882-0743
IS - 1367
ER -