Effect of silicon and heat-treatment temperature on the morphology and mechanical properties of silicon - Substituted hydroxyapatite

L. T. Bang, Kunio Ishikawa, R. Othman

研究成果: Contribution to journalArticle査読

39 被引用数 (Scopus)

抄録

The precipitation method was used to synthesize silicon-substituted hydroxyapatite with different Si contents of 0.4, 0.8 and 1.6 wt.% (0.4, 0.8 and 1.6Si-HA) using silicon acetate [Si(OCOCH3)4] as a Si source. As-synthesized hydroxyapatite (HA) and Si-HA powders/bulks were heat-treated at different temperatures of 1150, 1200 and 1250 °C for 1 h. Pure 0.4Si-HA and 1.6Si-HA were obtained after heat-treatment at all temperatures, whilst α-TCP phase was formed in the 0.8Si-HA sample after heat-treatment at 1250 °C. SEM observation clearly showed that the substitution of Si in HA inhibited the grain growth of Si-HA even at high heat-treatment temperatures (1200 or 1250 °C). The highest diametral tensile strength (DTS) of 15.93 MPa was obtained in the 1.6Si-HA sample after heat-treatment at 1250 °C.

本文言語英語
ページ(範囲)3637-3642
ページ数6
ジャーナルCeramics International
37
8
DOI
出版ステータス出版済み - 12 1 2011

All Science Journal Classification (ASJC) codes

  • Electronic, Optical and Magnetic Materials
  • Ceramics and Composites
  • Process Chemistry and Technology
  • Surfaces, Coatings and Films
  • Materials Chemistry

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