Examination of inverse Hall-Petch relation in nanostructured aluminum alloys by ultra-severe plastic deformation

Abbas Mohammadi, Nariman A. Enikeev, Maxim Yu Murashkin, Makoto Arita, Kaveh Edalati

研究成果: ジャーナルへの寄稿学術誌査読

19 被引用数 (Scopus)


To have an insight into the occurrence of inverse Hall-Petch relationship in ultrafine-grained (UFG) aluminum alloys produced by severe plastic deformation (SPD), ultra-SPD (i.e. inducing several ten thousand shear strains via high-pressure torsion, HPT) followed by aging is applied to an Al-La-Ce alloy. Average nanograin sizes of 40 and 80 nm are successfully achieved together with strain-induced Lomer-Cottrell dislocation lock formation and aging-induced semi-coherent Al11(La,Ce)3 precipitation. Analysis of hardening mechanisms in this alloy compared to SPD-processed pure aluminum with micrometer grain sizes, SPD-processed Al-based alloys with submicrometer grain sizes and ultra-SPD-processed Al-Ca alloy with nanograin sizes reveals the presence of two breaks in the Hall-Petch relationship. First, a positive up-break appears when the grain sizes decrease from micrometer to submicrometer which is due to extra hardening by solute-dislocation interactions. Second, a negative down-break and softening occur by decreasing the grain sizes from submicrometer to nanometer which is caused by weakening the dislocation hardening mechanism with minor contribution of the inverse Hall-Petch mechanism. Detailed analyses confirm that nanograin formation is not necessarily a solution for extra hardening of Al-based alloys and other accompanying strategies such as grain-boundary segregation and precipitation are required to overcome such a down-break and softening.

ジャーナルJournal of Materials Science and Technology
出版ステータス出版済み - 11月 20 2021

!!!All Science Journal Classification (ASJC) codes

  • セラミックおよび複合材料
  • 材料力学
  • 機械工学
  • ポリマーおよびプラスチック
  • 金属および合金
  • 材料化学


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