TY - JOUR
T1 - Extraction and recovery of limonoids with the supercritical carbon dioxide micro-bubble method
AU - Miyake, Masaki
AU - Shimoda, M.
AU - Osajima, Y.
AU - Inaba, Nobuya
AU - Ayano, Shigeru
AU - Ozaki, Yoshihiko
AU - Hasegawa, Shin
PY - 2000
Y1 - 2000
N2 - A new technique using supercritical carbon dioxide (SC-CO2) micro-bubble method to remove bitter limonoid aglycones from bitter juices has been developed. This procedure is also capable of isolating limonoid aglycones, purifying limonoid glucoside extracts obtained from citrus molasses and other sources, sterilizing the samples and inactivating enzymes in the samples. A pilot scale apparatus, which is capable of feeding a liquid sample and SC-CO2 continuously, successfully purified a limonoid glucoside extract isolated from mandarin. The yeild of limonoid glucosides in the SC-CO2 step was 97%. The product was practically odorless, tasteless and in an aceptic state.
AB - A new technique using supercritical carbon dioxide (SC-CO2) micro-bubble method to remove bitter limonoid aglycones from bitter juices has been developed. This procedure is also capable of isolating limonoid aglycones, purifying limonoid glucoside extracts obtained from citrus molasses and other sources, sterilizing the samples and inactivating enzymes in the samples. A pilot scale apparatus, which is capable of feeding a liquid sample and SC-CO2 continuously, successfully purified a limonoid glucoside extract isolated from mandarin. The yeild of limonoid glucosides in the SC-CO2 step was 97%. The product was practically odorless, tasteless and in an aceptic state.
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U2 - 10.1021/bk-2000-0758.ch007
DO - 10.1021/bk-2000-0758.ch007
M3 - Article
AN - SCOPUS:0041079348
SN - 0097-6156
VL - 758
SP - 96
EP - 106
JO - ACS Symposium Series
JF - ACS Symposium Series
ER -