Extractive alkylation and gas chromatographic analysis of sulfide

S. Kage, T. Nagata, K. Kimura, K. Kudo

研究成果: Contribution to journalArticle査読

49 被引用数 (Scopus)

抄録

A sensitive analysis of sulfide in blood was established, using an extractive alkylation technique. Pentafluorobenzyl bromide was used as the alkylating agent, tetradecyldimethyl-benzylammonium chloride as the phase-transfer catalyst, and potassium dihydrogenphosphate as the buffer to suppress the formation of sulfide. Mass fragmentography was used to identify the sulfide derivative and gas chromatography with an electron capture detector was used for quantitative determination, with the lowest limit of detection being about 0.01 μg/g. The blood level of rats exposed to hydrogen sulfide was also determined.

本文言語英語
ページ(範囲)217-222
ページ数6
ジャーナルJournal of Forensic Sciences
33
1
出版ステータス出版済み - 1 1 1988

All Science Journal Classification (ASJC) codes

  • 病理学および法医学
  • 遺伝学

フィンガープリント

「Extractive alkylation and gas chromatographic analysis of sulfide」の研究トピックを掘り下げます。これらがまとまってユニークなフィンガープリントを構成します。

引用スタイル