In-situ straining and time-resolved electron tomography data acquisition in a transmission electron microscope

S. Hata, S. Miyazaki, T. Gondo, K. Kawamoto, N. Horii, K. Sato, H. Furukawa, H. Kudo, H. Miyazaki, M. Murayama

研究成果: ジャーナルへの寄稿記事

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This paper reports the preliminary results of a new in-situ three-dimensional (3D) imaging system for observing plastic deformation behavior in a transmission electron microscope (TEM) as a directly relevant development of the recently reported straining-and-tomography holder [Sato K et al. (2015) Development of a novel straining holder for transmission electron microscopy compatible with single tilt-axis electron tomography. Microsc. 64: 369-375]. We designed an integrated system using the holder and newly developed straining and image-acquisition software and then developed an experimental procedure for in-situ straining and time-resolved electron tomography (ET) data acquisition. The software for image acquisition and 3D visualization was developed based on the commercially available ET software TEMographyTM. We achieved time-resolved 3D visualization of nanometer-scale plastic deformation behavior in a Pb-Sn alloy sample, thus demonstrating the capability of this system for potential applications in materials science.

元の言語英語
ページ(範囲)143-153
ページ数11
ジャーナルMicroscopy
66
発行部数2
DOI
出版物ステータス出版済み - 4 1 2017

    フィンガープリント

All Science Journal Classification (ASJC) codes

  • Structural Biology
  • Instrumentation
  • Radiology Nuclear Medicine and imaging

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