Preparation of glycidyl celluloses from completely allylated methylcellulose and tri‐O‐allylcellulose

Tetsuo Kondo; Atsushi Ishizu; Junzo Nakano

doi:10.1002/app.1989.070371017

Preparation of glycidyl celluloses from completely allylated methylcellulose and tri‐O‐allylcellulose

Tetsuo Kondo, Atsushi Ishizu, Junzo Nakano

研究成果: Contribution to journal › Article › 査読

10 被引用数 (Scopus)

抄録

Glycidyl celluloses were prepared from completely allylated methylcellulose and tri‐O‐allylcellulose with m‐chloroperbenzoic acid in homogeneous chloroform solutions. The degrees of substitution (DS) by epoxy groups were 0.60 and 1.33 for the products prepared from allylated methylcellulose and tri‐O‐allylcellulose, respectively. They were soluble in not only many organic solvents, but also methanol‐water mixtures [more than 70% (v/v)]. These products were characterized by infrared spectroscopy (IR), ¹³C‐NMR spectroscopy, and gel permeation chromatography (GPC).

本文言語	英語
ページ（範囲）	3003-3009
ページ数	7
ジャーナル	Journal of Applied Polymer Science
巻	37
号	10
DOI	https://doi.org/10.1002/app.1989.070371017
出版ステータス	出版済み - 5 20 1989
外部発表	はい

All Science Journal Classification (ASJC) codes

Chemistry(all)
Surfaces, Coatings and Films
Polymers and Plastics
Materials Chemistry

文献へのアクセス

10.1002/app.1989.070371017

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引用スタイル

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AU - Ishizu, Atsushi

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Y1 - 1989/5/20

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AB - Glycidyl celluloses were prepared from completely allylated methylcellulose and tri‐O‐allylcellulose with m‐chloroperbenzoic acid in homogeneous chloroform solutions. The degrees of substitution (DS) by epoxy groups were 0.60 and 1.33 for the products prepared from allylated methylcellulose and tri‐O‐allylcellulose, respectively. They were soluble in not only many organic solvents, but also methanol‐water mixtures [more than 70% (v/v)]. These products were characterized by infrared spectroscopy (IR), 13C‐NMR spectroscopy, and gel permeation chromatography (GPC).

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