Preparation of glycidyl celluloses from completely allylated methylcellulose and tri‐O‐allylcellulose

Tetsuo Kondo, Atsushi Ishizu, Junzo Nakano

研究成果: ジャーナルへの寄稿記事

8 引用 (Scopus)

抄録

Glycidyl celluloses were prepared from completely allylated methylcellulose and tri‐O‐allylcellulose with m‐chloroperbenzoic acid in homogeneous chloroform solutions. The degrees of substitution (DS) by epoxy groups were 0.60 and 1.33 for the products prepared from allylated methylcellulose and tri‐O‐allylcellulose, respectively. They were soluble in not only many organic solvents, but also methanol‐water mixtures [more than 70% (v/v)]. These products were characterized by infrared spectroscopy (IR), 13C‐NMR spectroscopy, and gel permeation chromatography (GPC).

元の言語英語
ページ(範囲)3003-3009
ページ数7
ジャーナルJournal of Applied Polymer Science
37
発行部数10
DOI
出版物ステータス出版済み - 5 20 1989

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Methylcellulose
Gel permeation chromatography
Chlorine compounds
Cellulose
Organic solvents
Infrared spectroscopy
Substitution reactions
Spectroscopy
Acids
Chloroform

All Science Journal Classification (ASJC) codes

  • Chemistry(all)
  • Surfaces, Coatings and Films
  • Polymers and Plastics
  • Materials Chemistry

これを引用

Preparation of glycidyl celluloses from completely allylated methylcellulose and tri‐O‐allylcellulose. / Kondo, Tetsuo; Ishizu, Atsushi; Nakano, Junzo.

:: Journal of Applied Polymer Science, 巻 37, 番号 10, 20.05.1989, p. 3003-3009.

研究成果: ジャーナルへの寄稿記事

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AB - Glycidyl celluloses were prepared from completely allylated methylcellulose and tri‐O‐allylcellulose with m‐chloroperbenzoic acid in homogeneous chloroform solutions. The degrees of substitution (DS) by epoxy groups were 0.60 and 1.33 for the products prepared from allylated methylcellulose and tri‐O‐allylcellulose, respectively. They were soluble in not only many organic solvents, but also methanol‐water mixtures [more than 70% (v/v)]. These products were characterized by infrared spectroscopy (IR), 13C‐NMR spectroscopy, and gel permeation chromatography (GPC).

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