Separation of fullerenes with novel stationary phases in microcolumn high performance liquid chromatography

Yoshihiro Saito, Hatsuichi Ohta, Hideo Nagashima, Kenji Itoh, Kiyokatsu Jinno

研究成果: Contribution to journalArticle査読

18 被引用数 (Scopus)

抄録

Newly designed bonded phases have been synthesized and evaluated for the separation of fullerene molecules. Further investigations about the retention behaviour of fullerenes with these phases have been carried out systematically. In this study we describe the separation of fullerenes with novel bonded stationary phases in microcolumn high performance liquid chromatography (micro-HPLC) and also propose the basic separation mechanism of those molecules obtained from the preliminary chromatographic observations. The results indicate that the octadecyldiphenyl bonded silica phases, which have been synthesized from oetadecyldiphenylehlorosilane as the silanization reagent, possess a better retentivity for fullerenes than the octadecyldimethylsilica phase (i.e. monomeric ODS phase) having a similar surface coverage value.

本文言語英語
ページ(範囲)1897-1908
ページ数12
ジャーナルJournal of Liquid Chromatography
18
10
DOI
出版ステータス出版済み - 6 1 1995
外部発表はい

All Science Journal Classification (ASJC) codes

  • Molecular Medicine

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