Simple Apparatus for Adding Small Amounts of Powder Materials under an Inert Atmosphere

Milandip Karak, Yohei Joh, Khamid U. Khodjaniyazov, Shamansur S. Sagdullaev, Tohru Oishi, Kohei Torikai

研究成果: ジャーナルへの寄稿記事

抄録

Addition of reactants under an inert atmosphere is a fundamental but extremely important technique in synthetic chemistry. Although this is achievable in many cases by using a glove box or a Schlenk-and-syringe technique, the direct addition of powder (solid) materials without contamination by air or moisture has been difficult, especially in the later stages of a reaction. Here, we offer a simple and small apparatus to realize powder addition with easy handling. Use of this apparatus permitted one-pot glycosylation reactions that required extremely dry conditions to be performed in a highly reproducible manner.

元の言語英語
ページ(範囲)2058-2061
ページ数4
ジャーナルSynlett
30
発行部数18
DOI
出版物ステータス出版済み - 1 1 2019

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Powders
Glycosylation
Syringes
Contamination
Moisture
Air

All Science Journal Classification (ASJC) codes

  • Organic Chemistry

これを引用

Simple Apparatus for Adding Small Amounts of Powder Materials under an Inert Atmosphere. / Karak, Milandip; Joh, Yohei; Khodjaniyazov, Khamid U.; Sagdullaev, Shamansur S.; Oishi, Tohru; Torikai, Kohei.

:: Synlett, 巻 30, 番号 18, 01.01.2019, p. 2058-2061.

研究成果: ジャーナルへの寄稿記事

Karak, Milandip ; Joh, Yohei ; Khodjaniyazov, Khamid U. ; Sagdullaev, Shamansur S. ; Oishi, Tohru ; Torikai, Kohei. / Simple Apparatus for Adding Small Amounts of Powder Materials under an Inert Atmosphere. :: Synlett. 2019 ; 巻 30, 番号 18. pp. 2058-2061.
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