Synthesis and Rietveld analysis for CoSb3 compounds prepared by Sb self-flux method

Takeshi Souma, Michitaka Ohtaki

    研究成果: Chapter in Book/Report/Conference proceedingConference contribution

    2 被引用数 (Scopus)

    抄録

    High purity CoSb3 bulk crystals have been successfully synthesized by Sb self-flux method and a relation between reaction conditions and chemical composition on the method has been systematically analyzed by powder XRD study using the Rietveld analysis. Sb self flux method at 923 K using 100 mesh Co elements can directly provide a single phase CoSb3 bulk crystal in a brief time of 10 h. Advantages of Sb self-flux methods will be discussed compared with other preparation methods.

    本文言語英語
    ホスト出版物のタイトルProceedings - ICT'05
    ホスト出版物のサブタイトル24th International Conference on Thermoelectrics
    ページ121-124
    ページ数4
    DOI
    出版ステータス出版済み - 2005
    イベントICT'05: 24th International Conference on Thermoelectrics - Clemson, SC, 米国
    継続期間: 6 19 20056 23 2005

    出版物シリーズ

    名前International Conference on Thermoelectrics, ICT, Proceedings
    2005

    その他

    その他ICT'05: 24th International Conference on Thermoelectrics
    Country米国
    CityClemson, SC
    Period6/19/056/23/05

    All Science Journal Classification (ASJC) codes

    • Engineering(all)

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